Benzoyl chloride → HCID 54037041, compound

HRID 2050864Notes

Reaction equation

HRID 2050864 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:25])[O:17][CH2:18]C3CCCCO3)[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[C:26](Cl)(=[O:33])[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1>>[C:26]([N:25]=[C:16]([N:7]1[CH2:8][C:9]2[CH:15]=[CH:14][CH:13]=[CH:12][C:10]=2[C:11]2[CH:1]=[CH:2][CH:3]=[CH:4][C:5]=2[CH2:6]1)[O:17][CH:18]1[CH2:29][CH2:28][CH2:27][CH2:26][O:33]1)(=[O:33])[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1

Participants

3

Reactant 2

HCID 7412Benzoyl chlorideHCID 703673312-tetrahydro-2H-pyranylmethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate

Product 1

HCID 54037041HCID 54037041, compound

Procedure

starting from 2-tetrahydro-2H-pyranylmethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and benzoyl chloride, there is obtained tetrahydro-2H-pyran-2-yl N-(benzoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6 carboximidate, m.p, 114.5°-117° C.;

Sources & evidence

ORD record
ord-ebcf98ef296e44d9b21d7b763e48a273
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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