Benzoyl chloride → HCID 19833941, compound

HRID 2050865Notes

Reaction equation

[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:23])[O:17][CH2:18][CH2:19][C:20]#[C:21][CH3:22])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[C:24](Cl)(=[O:31])[C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1>>[C:24]([N:23]=[C:16]([N:7]1[CH2:6][C:5]2[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=2[C:10]2[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=2[CH2:8]1)[O:17][CH2:18][CH2:19][C:20]#[C:21][CH3:22])(=[O:31])[C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1

Participants

Reactant 2

HCID 7412Benzoyl chloride

HCID 19833982HCID 19833982, compound

Product 1

HCID 19833941HCID 19833941, compound

Procedure

starting from 3-pentynyl 5,7-dihydro-6H-dibenz[c,e]-azepine-6-carboximidate and benzoyl chloride, there is obtained 3-pentynyl N-(benzoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a syrup, mass spectrum m/e: M+ 408 (3), 407 (4), 341 (8), 194 (100), 105 (57);

Sources & evidence

ORD record: ord-66f4cd3b5982462baedf39a1f77339ed
Source dataset: uspto-grants-1991_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05015640

Reaction notes

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