1,3-Benzodioxole-5-carbonyl chloride → HCID 19833960, compound

HRID 2050866Notes

Reaction equation

HRID 2050866 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:20])[O:17][CH2:18][CH3:19])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[CH2:21]1[O:32][C:31]2[CH:30]=[CH:29][C:25]([C:26](Cl)=[O:27])=[CH:24][C:23]=2[O:22]1>>[CH2:21]1[O:32][C:31]2[CH:30]=[CH:29][C:25]([C:26]([N:20]=[C:16]([N:7]3[CH2:6][C:5]4[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=4[C:10]4[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=4[CH2:8]3)[O:17][CH2:18][CH3:19])=[O:27])=[CH:24][C:23]=2[O:22]1

Participants

3

Reactant 2

HCID 27347491,3-Benzodioxole-5-carbonyl chlorideHCID 19833914ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate

Product 1

HCID 19833960HCID 19833960, compound

Procedure

starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and 3,4-methylenedioxybenzoyl chloride, there is obtained ethyl N-(3,4-methylenedioxybenzoyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as a syrup, mass spectrum m/e: M+ 414 (5), 385 (7), 194 (100), 149 (33);

Sources & evidence

ORD record
ord-e67ee0b293f34f9a9ebebfe00474c3bb
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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