3-Methylbenzoyl chloride → HCID 19833963, compound

HRID 2050867Notes

Reaction equation

HRID 2050867 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:20])[O:17][CH2:18][CH3:19])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[C:21]1([CH3:30])[CH:26]=[CH:25][CH:24]=[C:23]([C:27](Cl)=[O:28])[CH:22]=1>>[C:21]1([CH3:30])[CH:26]=[CH:25][CH:24]=[C:23]([C:27]([N:20]=[C:16]([N:7]2[CH2:6][C:5]3[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=3[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8]2)[O:17][CH2:18][CH3:19])=[O:28])[CH:22]=1

Participants

3

Reactant 2

HCID 743753-Methylbenzoyl chlorideHCID 19833914ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate

Product 1

HCID 19833963HCID 19833963, compound

Procedure

starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and m-toluoyl chloride, there is obtained ethyl N-(m-toluoyl)-5,7-dihydro-6H-dibenz[c,e]azepin-6-carboximidate m.p. 102°-105° C.;

Sources & evidence

ORD record
ord-b454019579cc4c119a8de1d8bc420cf8
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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