Allyl chloroformate → HCID 53978042, compound

HRID 2050875Notes

Reaction equation

HRID 2050875 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:20])[O:17][CH2:18][CH3:19])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.Cl[C:22]([O:24][CH2:25][CH:26]=[CH2:27])=[O:23]>>[CH2:25]([O:24][C:22]([N:20]=[C:16]([N:7]1[CH2:6][C:5]2[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=2[C:10]2[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=2[CH2:8]1)[O:17][CH2:18][CH3:19])=[O:23])[CH:26]=[CH2:27]

Participants

3

Reactant 2

HCID 18052Allyl chloroformateHCID 19833914ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate

Product 1

HCID 53978042HCID 53978042, compound

Procedure

starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and allyl chloroformate, there is obtained ethyl N-allyloxycarbonyl-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate, m.p. 76°-77.5° C.;

Sources & evidence

ORD record
ord-9d7de9c47c414a9ab1e68a3fc933b5da
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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