2-Chloroethyl chloroformate → HCID 67929416, compound

HRID 2050876Notes

Reaction equation

HRID 2050876 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:20])[O:17][CH2:18][CH3:19])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.Cl[C:22]([O:24][CH2:25][CH2:26][Cl:27])=[O:23]>>[Cl:27][CH2:26][CH2:25][O:24][C:22]([N:20]=[C:16]([N:7]1[CH2:6][C:5]2[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=2[C:10]2[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=2[CH2:8]1)[O:17][CH2:18][CH3:19])=[O:23]

Participants

3

Reactant 2

HCID 123052-Chloroethyl chloroformateHCID 19833914ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate

Product 1

HCID 67929416HCID 67929416, compound

Procedure

starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and 2-chloroethyl chloroformate, there is obtained ethyl N-(2-chloroethoxycarbonyl)-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate as an oil, mass spectrum m/e: M+ 372 (4), 343 (12), 293 (10), 263 (72), 194 (100), 178 (86), 165 (79);

Sources & evidence

ORD record
ord-d23334d15cc34aeaaa225c836a78df6a
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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