4-Chlorophenyl Isocyanate → HCID 67929414, compound

HRID 2050882Notes

Reaction equation

HRID 2050882 reaction equation
[CH:1]1[C:11]2[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8][N:7]([C:16](=[NH:20])[O:17][CH2:18][CH3:19])[CH2:6][C:5]=2[CH:4]=[CH:3][CH:2]=1.[Cl:21][C:22]1[CH:27]=[CH:26][C:25]([N:28]=[C:29]=[O:30])=[CH:24][CH:23]=1>>[Cl:21][C:22]1[CH:27]=[CH:26][C:25]([NH:28][C:29]([N:20]=[C:16]([N:7]2[CH2:6][C:5]3[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=3[C:10]3[CH:12]=[CH:13][CH:14]=[CH:15][C:9]=3[CH2:8]2)[O:17][CH2:18][CH3:19])=[O:30])=[CH:24][CH:23]=1

Participants

3

Reactant 2

HCID 76934-Chlorophenyl IsocyanateHCID 19833914ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate

Product 1

HCID 67929414HCID 67929414, compound

Procedure

starting from ethyl 5,7-dihydro-6H-dibenz[c,e]-azepine-6-carboximidate and p-chlorophenyl isocyanate, there is obtained ethyl N-[(p-chlorophenyl)carbamoyl]-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate, m.p. 154°-156° C.;

Sources & evidence

ORD record
ord-0a8096d4aa7843b1a050fc432a97c27e
Source dataset
uspto-grants-1991_05
Patent number
US05015640

Reaction notes

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