HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-(Trifluoromethoxy)phenyl isocyanate → ethyl N-{[p-(trifluoromethoxy)-phenyl]carbamoyl}-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-(Trifluoromethoxy)phenyl isocyanate | HCID 92298 | — |
| Reactant | ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6carboximidate | HCID 19833914 | — |
| Product | ethyl N-{[p-(trifluoromethoxy)-phenyl]carbamoyl}-5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate | HCID 67929433 | — |
Reaction Steps
starting from ethyl 5,7-dihydro-6H-dibenz[c,e]azepine-6-carboximidate and p-(trifluoromethoxy)-phenyl isocyanate, there is obtained ethyl N-{[p-(trifluoromethoxy)-phenyl]carbamoyl}-5,7-dihydro-6H-dibenz[c,e]azepine-6 -carboximidate, m.p. 129°-130° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05015640 |
| Source dataset | uspto-grants-1991_05 |
| ORD ID | ord-c3a0d783706c40a8aa7b3990f3de05c1 |
| Source note | uspto-grants-1991_05 |