HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenylcyclobutylamine → N-(2, 6-diethylphenyl)-N'-(1-phenylcyclobutyl)urea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenylcyclobutylamine | HCID 152214 | — |
| Reactant | 2,6-Diethylphenyl isocyanate | HCID 5153183 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | N-(2, 6-diethylphenyl)-N'-(1-phenylcyclobutyl)urea | HCID 15172041 | 79.4% |
Reaction Steps
To a solution of 1-phenylcyclobutyl amine (1.0, 0.0057 mole) in 30 ml of ethylacetate, 2,6-diethylphenylisocyanate (0.84 g, 0.0057 mole) is added and the reaction mixture is stirred at room temperature for 20 hours. Precipitated solid is filtered, washed with ethylacetate and dried yielding 1.46 gm of N-(2, 6-diethylphenyl)-N'-(1-phenylcyclobutyl)urea having a melting point of 227°-230° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05015644 |
| Source dataset | uspto-grants-1991_05 |
| ORD ID | ord-a81ec2e9556a4fc0883d77fe2428c888 |
| Source note | uspto-grants-1991_05 |