Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Methoxyethanol | HCID 8019 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 5,6-Dinitro-1,3-benzodioxole | HCID 611325 | — |
| Product | HCID 13750863 | HCID 13750863 | — |
Reaction Steps
0.2 mol (13.2 g) of potassium hydroxide pellets (85%) is added to 100 ml of ethylene glycol monomethyl ether which has been heated beforehand to 45° C. 0.1 mol (21.2 g) of 4,5-methylenedioxy-1,2-dinitrobenzene, prepared according to Example 1, is added to this solution in the course of 5 minutes. The heating is maintained for 1 hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05015769 |
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| Source dataset | uspto-grants-1991_05 |
|---|
| ORD ID | ord-741640b71ae94a91a7772110b1ba5da5 |
|---|
| Source note | uspto-grants-1991_05 |
|---|
