HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2051047Generated: October 31, 2026
Methanesulfonic Acid → HCID 19834656, compound
https://huagongshe.com/reaction/2051047
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | 1,2-Diethylbenzene | HCID 8657 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Product | HCID 19834656 | HCID 19834656 | 12% |
Reaction Steps
An isomeric mixture of diethyl benzene (268.44 g, 2.0 moles), anhydrous methane sulfonic acid (96.1 g, 1.0 mole) and phosphorus oxychloride (25.6 g, 2.17 moles) were heated at 90° C. with stirring for 8 hours. Treatment of the reaction mixture after cooling was the same as in Example 1 and 25 g (12% yield) of methyl diethylphenyl sulfone was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05015775 |
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| Source dataset | uspto-grants-1991_05 |
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| ORD ID | ord-76224014096844bfb98d5e2f0d0f094a |
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| Source note | uspto-grants-1991_05 |
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