反应详情

In a 100 ml three-necked flask, under a nitrogen environment, are placed 2 g of 1-acetoxyadamantane and 20 ml of n-heptane. After total dissolution, 0.5 g of concentrated sulfuric acid is added drop by drop. At a temperature of approximately 20.C, 1.71 g of methyl 4-methoxybenzoate is added slowly and agitated for 48 hours. The solid obtained is filtered with sintered glass and washed with water until neutrality is reached. After drying in a vacuum oven for 24 hours at 25 C, one recovered 2 g of expected raw product (Melting point: 136°-137° C.).

1. customIn a 100 ml three-necked flask, under a nitrogen environment, are placed
2. additionis added drop by drop
3. customThe solid obtained
4. filtrationis filtered with sintered glass
5. washwashed with water until neutrality
6. customAfter drying in a vacuum oven for 24 hours at 25 C, one
7. customrecovered 2 g of expected raw product (Melting point: 136°-137° C.)