HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → 2-Chloro-alpha-methyl-3-nitrobenzenemethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | 1-(2-Chloro-3-nitrophenyl)ethanone | HCID 12463885 | — |
| Product | 2-Chloro-alpha-methyl-3-nitrobenzenemethanol | HCID 15735720 | 83.4% |
Reaction Steps
According to the procedure of Example 3, 1-(2-chloro-3-nitrophenyl)ethanone (9.0 g, 44.6 mmol) is reacted with sodium borohydride (0.84 g, 22.3 mmol) to give 2-chloro-α-methyl-3-nitrobenzenemethanol (7.5 g, 83%), mp=62-64° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05017604 |
| Source dataset | uspto-grants-1991_05 |
| ORD ID | ord-196ff7a0f53c4d9fa3b2fd6c61ddd9e1 |
| Source note | uspto-grants-1991_05 |