Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Allyltrimethylsilane → 4,5-Dichloro-4,5,5-trifluoropent-1-ene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Allyltrimethylsilane | HCID 69808 | — |
| 반응물 | 1,2-Dichloro-1,1,2-trifluoro-2-iodoethane | HCID 78981 | — |
| 생성물 | 4,5-Dichloro-4,5,5-trifluoropent-1-ene | HCID 13128776 | — |
반응 단계
A mixture of 279 mg (1.0 mmol) of 1,2-dichloro-1-iodotrifluoroethane and 114 mg (1.0 mmol) of allyltrimethylsilane was sealed in a Pyrex glass tube and externally radiated with a high pressure mercury lamp (400 W) in an ice-bath for 3 hours to obtain 4,5-dichloro-4,5,5-trifluoro-1-pentene (Compound 39) in a yield of 60%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05017718 |
| 출처 데이터셋 | uspto-grants-1991_05 |
| ORD ID | ord-7ea2b75682744179b1ab37e580e462ce |
| 출처 메모 | uspto-grants-1991_05 |