HuagongsheHuagongshe Chemistry Print Report · For research reference only
Maleic Acid → HCID 67900100, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Maleic Acid | HCID 444266 | — |
| Reactant | HCID 54074507 | HCID 54074507 | — |
| Product | HCID 67900100 | HCID 67900100 | 64.1% |
Reaction Steps
The filtrate from the hydrogenation of 1-(5-fluoro-1-naphthalenyl)-3-(5-methyl-1H-imidazol-4-yl)-2-propen-1-one (1.01 g) was treated with maleic acid (418 mg) and the resultant solution was evaporated to dryness to give a solid. This was recrystallised from methanol/ethyl acetate to give the title compound (920 mg), m.p. 138°-140°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05019586 |
| Source dataset | uspto-grants-1991_05 |
| ORD ID | ord-4131b106dc394133bd228379115cf108 |
| Source note | uspto-grants-1991_05 |