HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,7-Octadien-3-ol → 1,7-octadien-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,7-Octadien-3-ol | HCID 545738 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 1,7-octadien-3-one | HCID 11804752 | — |
Reaction Steps
To 100 cc of carbon tetrachloride containing 3.1 g of 1,7-octadien-3-ol (III) was added 10 g of active manganese dioxide, and the mixture was stirred at room temperature for 4 days. After filtration, the solvent (filtrate) was distilled off at a reduced pressure of 20 to 30 mm Hg to obtain 2 g of 1,7-octadien-3-one at 30°-32° C./4 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04181683 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-cb578c10fa4a46c7af9aa245df9633c2 |
| Source note | uspto-grants-1980_01 |