HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenepropanoic acid → Isopropyl 3-phenylpropionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenepropanoic acid | HCID 107 | — |
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | Isopropyl 3-phenylpropionate | HCID 347496 | 94% |
Reaction Steps
To a mixture of 3-phenylpropionic acid (15.0 g) and isopropanol (6.61 g) in pyridine (30 ml) perchloric acid (0.150 g) and DCC (24.8 g) are added. After stirring at room temperature for 24 h acetic acid (10 ml) is added, and the reaction mixture is worked-up as described in Example 1 to give a 94% yield of isopropyl 3-phenylpropionate (b. p., see Example 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04181669 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-e5f6df706afd463dba6bb5dfe697c2dd |
| Source note | uspto-grants-1980_01 |