HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzenesulfonic acid → HCID 20377982, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzenesulfonic acid | HCID 6925 | — |
| Reactant | HCID 12798409 | HCID 12798409 | — |
| Solvent | 1-Propanol | HCID 1031 | — |
| Product | HCID 20377982 | HCID 20377982 | — |
Reaction Steps
The compound was prepared by transesterification of 2.9 g (0.01 mol) of 1-benzhydryl-5-methoxycarbonyl-imidazole of Example 8. To this end it was refluxed for some time in 100 cc of propanol and in the presence of catalytic amounts of toluene sulfonic acid. The colorless crystals obtained had a melting point of 81° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182624 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-d9c53239bb2346e9bfba765b60a243e9 |
| Source note | uspto-grants-1980_01 |