HuagongsheHuagongshe Chemistry Print Report · For research reference only
Vinyl Chloride → HCID 178527065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Vinyl Chloride | HCID 6338 | — |
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | HCID 131711413 | HCID 131711413 | — |
| Product | HCID 178527065 | HCID 178527065 | 67.6% |
Reaction Steps
20 g of vinyl chloride and 20 g of chlorine are passed into 20 g of phosphoric acid monopropyl ester-dichloride, the reaction temperature being kept between 0° C. and +10° C. by cooling. Working up by distillation gives 16 g (=62.5% of theory) of phosphonic acid (1,2-dichloroethyl) ester-dichloride, which has a boiling range of 56°-60° C./0.1 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182733 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-fddd581d4e594a758a2ad9ebd682d002 |
| Source note | uspto-grants-1980_01 |