HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron trifluoride etherate → HCID 20378290, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron trifluoride etherate | HCID 8000 | — |
| Reactant | 1,2-Ethanedithiol | HCID 10902 | — |
| Reactant | HCID 20378297 | HCID 20378297 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20378290 | HCID 20378290 | — |
Reaction Steps
17 g [0.063 mol] of 2-(4-formylbutyl)-3-oxo-cyclopentane-carbonitrile were dissolved in 200 ml of toluene and stirred for 30 minutes at room temperature with [0.08 mol]=6.7 ml of 1,2-ethanedithiol and 2 ml of boron trifluoride etherate, washed with water and sodium bicarbonate solution, dried over sodium sulfate and concentrated. 15.6 g of a light color oil were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182773 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-27230b4a29654bf381fc3d4497f276d9 |
| Source note | uspto-grants-1980_01 |