HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Naphthol → 2-(2-Naphthoxy)ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Naphthol | HCID 8663 | — |
| Reactant | 2-Bromoethanol | HCID 10898 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-(2-Naphthoxy)ethanol | HCID 7131 | — |
Reaction Steps
A solution of 14.4 g of 2-naphthol, 12.1 g of 2-bromoethanol and 5.9 g of sodium methoxide in 100 ml of ethanol is allowed to stand two days at room temperature. The solvent is removed under vacuum and the residue extracted with ether. The ether extract is washed with water dried (magnesium sulfate) and the solvent removed under vacuum to give crystals, mp 65°-70° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182776 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-d992e7f9e0c844f58474c5af489c04d0 |
| Source note | uspto-grants-1980_01 |