HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 20378398, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 1-Hexanol, 6-phenoxy- | HCID 12293215 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 20378398 | HCID 20378398 | — |
Reaction Steps
To a chilled (-2° C.) mixture of 9.7 g of 6-(phenoxy)-1-hexanol in 250 ml of dichloromethane containing 11.1 g of triethylamine is added 6.95 g of methanesulfonyl chloride. The product is isolated as described in Example 2 to give the product as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182776 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-c5f565545d364156a583b91c352b23c0 |
| Source note | uspto-grants-1980_01 |