HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenoxybenzoic acid → 3-Phenoxybenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenoxybenzoic acid | HCID 19539 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 3-Phenoxybenzoyl chloride | HCID 2760341 | — |
Reaction Steps
Added portionwise 25 g (0.12 mole) of 3-phenoxybenzoic acid, to 125 ml of thionyl chloride, then heated at reflux for 2 hrs. The solution was distilled to remove the excess thionyl chloride. Added 200 ml of AR toluene and evaporated in vacuo to give 23 g of red liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04182881 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-ce78b5fbdafc424fbfbe540450565e3f |
| Source note | uspto-grants-1980_01 |