HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → alpha-(2-Acetoxy-5-sulfophenylazo)acetoacetanilide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | alpha-(2-Hydroxy-5-sulfophenylazo)acetoacetanilide | HCID 135839437 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | alpha-(2-Acetoxy-5-sulfophenylazo)acetoacetanilide | HCID 23336111 | — |
Reaction Steps
α-(2-hydroxy-5-sulfophenylazo)acetoacetanilide (40 g) was dissolved in boiling pyridine (750 ml) and acetic anhydride (100 ml) added. Some material precipitated while the reaction mixture was hot. After being cooled, the product was filtered off and dried. Yield: 38 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04183755 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-dc614a1fcf76419a9bcd9dce6a459e38 |
| Source note | uspto-grants-1980_01 |