HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2052372Generated: October 27, 2026
3-Methyl-1-butene → 5-Hydroxy-2-methyl-6,6,6-trifluoro-5-trifluoromethylhex-2-ene
https://huagongshe.com/reaction/2052372
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 3-Methyl-1-butene | HCID 11239 | — |
| Reactant | Hexafluoroacetone | HCID 12695 | — |
| Product | 5-Hydroxy-2-methyl-6,6,6-trifluoro-5-trifluoromethylhex-2-ene | HCID 12783437 | — |
Reaction Steps
A stirred mixture of hexafluoroacetone (235 g) and 3-methylbut-1-ene (100 g) was heated at 125° C. under a pressure of 17 atmospheres for a period of 20 hours. Distillation of the product mixture under reduced pressure yielded 5-hydroxy-2-methyl-6,6,6-trifluoro-5-trifluoromethylhex-2-ene as a mobile colourless liquid, b.p. 43° C./15 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04183948 |
|---|
| Source dataset | uspto-grants-1980_01 |
|---|
| ORD ID | ord-364be3521c204f6bb7df84aca51f0cf7 |
|---|
| Source note | uspto-grants-1980_01 |
|---|
