HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Hydroxide → 2-chloro-3,5-dinitrobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 12897330 | HCID 12897330 | — |
| Product | 2-chloro-3,5-dinitrobenzamide | HCID 235627 | 94% |
Reaction Steps
A mixture of 37.0 gm. (0.14 mole) of 2-chloro-3,5-dinitrobenzoyl chloride and 100 ml. of concentrated ammonium hydroxide is placed in a mortar, ground for ten minutes and allowed to stand for one hour. The yellow precipitate is removed by filtration and washed with water. There is obtained 32.3 gm (94%) of material melting at 181-3°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04186127 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-0483ba9e01fd4240a060baa768aa6ea7 |
| Source note | uspto-grants-1980_01 |