HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → Behenyl Alcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Docosanoic Acid | HCID 8215 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Behenyl Alcohol | HCID 12620 | 26.1% |
Reaction Steps
4 g of docosanoic acid are dissolved in 150 ml of anhydrous ether. LeAlH4 is progressively introduced. On completion of the reaction, 150 ml of an aqueous solution of 1 N acetic acid are introduced. The ethereal phase is then separated off, decanted and dried. Rectification in vacuo gives approximately 1 g of 1-docosanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04186211 |
| Source dataset | uspto-grants-1980_01 |
| ORD ID | ord-958ed5024c994d6ba208cd81d304a2ea |
| Source note | uspto-grants-1980_01 |