3,4-Dichloroaniline → HCID 20376419, compound

HRID 2052720Notes

Reaction equation

HRID 2052720 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:6]=[CH:7][C:8]=1[Cl:9])[NH2:5].Cl.Cl[CH2:12][CH2:13][N:14]([CH3:16])[CH3:15].C(=O)([O-])[O-].[Na+].[Na+]>C1(C)C=CC=CC=1>[CH3:15][N:14]([CH3:16])[CH2:13][CH2:12][NH:5][C:4]1[CH:6]=[CH:7][C:8]([Cl:9])=[C:2]([Cl:1])[CH:3]=1

Participants

5

Reactant 3

HCID 72573,4-DichloroanilineHCID 10340Sodium CarbonateHCID 11636816N,N-Dimethylaminoethyl chloride hydrochloride

Product 1

HCID 20376419HCID 20376419, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

In the manner given in Example 5, 3,4-dichloroaniline, 1-chloro-2-dimethylaminoethane hydrochloride and sodium carbonate are heated in toluene to give N,N-dimethyl-N'-(3,4-dichlorophenyl)ethylenediamine.

Sources & evidence

ORD record
ord-b0b7b4c08eac4f4e8ac79cb9defdeaf6
Source dataset
uspto-grants-1980_01
Patent number
US04186208

Reaction notes

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