HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2052780Generated: October 31, 2026
4-Hydroxybenzaldehyde → p-Dodecyloxybenzaldehyde
https://huagongshe.com/reaction/2052780
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Hydroxybenzaldehyde | HCID 126 | — |
| Reactant | 1-Bromododecane | HCID 8919 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | p-Dodecyloxybenzaldehyde | HCID 141069 | 99.8% |
Reaction Steps
4-Hydroxybenzaldehyde (673 mg, 5.5 mmol), 1-bromododecane (1.25 g, 5 mmol) and potassium carbonate (859 mg, 6.22 mmol) were added to dimethylformamide (3 ml), and they were stirred at 65° C. for 18 hours. After the completion of the reaction followed by the extraction with ethyl acetate, 4-dodecyloxybenzaldehyde (yield: 1.45 g, 99%) was obtained in the form of white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07326701B2 |
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| Source dataset | uspto-grants-2008_02 |
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| ORD ID | ord-56cbc2e31fe2402ca7a24e3159782ab4 |
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| Source note | uspto-grants-2008_02 |
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