HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methylbenzyl isocyanate → HCID 178425245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methylbenzyl isocyanate | HCID 2733387 | — |
| Reactant | HCID 178511294 | HCID 178511294 | — |
| Product | HCID 178425245 | HCID 178425245 | — |
Reaction Steps
cis-1-{3-[4-Amino-5-(3-benzyloxy-phenyl)-pyrrolo[2,3-d]pyrimidin-7-yl]-cyclobutylmethyl}-3-(3-methyl-benzyl)-urea is prepared as described in Example 26 using cis-7-(3-aminomethyl-cyclobutyl)-5-(3-benzyloxy-phenyl)-7H-pyrrolo[2,3-d]pyrimidin-4-ylamine and 3-methylbenzyl isocyanate (Aldrich, Buchs, Switzerland). Analytical HPLC: tR=7.45 min (Grad 2); ES-MS: m/eo=546.9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326699B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-29db67ce24e340639c688d46c68541c1 |
| Source note | uspto-grants-2008_02 |