HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethoxyacetic acid → HCID 178468080, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethoxyacetic acid | HCID 12301 | — |
| Reactant | HCID 178511295 | HCID 178511295 | — |
| Product | HCID 178468080 | HCID 178468080 | — |
Reaction Steps
trans-N-{3-[4-Amino-5-(3-benzyloxy-phenyl)-pyrrolo[2,3-d]pyrimidin-7-yl]-cyclobutylmethyl}-2-ethoxy-acetamide is prepared starting from trans-7-(3-aminomethyl-cyclobutyl)-5-(3-benzyloxy-phenyl)-7H-pyrrolo[2,3-d]pyrimidin-4-ylamine and ethoxy-acetic acid (Fluka, Buchs, Switzerland) according to a procedure known in the art (M. Bodanszky in Principles of Peptide Synthesis, Akad.-Verlag, 1984). Analytical HPLC: tR=7.07 min (Grad 2); ES-MS: m/eo=486.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326699B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-e186071c29c94ffa861c80c987f182f4 |
| Source note | uspto-grants-2008_02 |