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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2053010Generated: October 30, 2026

Ethoxyacetic acid → HCID 178468080, compound

https://huagongshe.com/reaction/2053010

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthoxyacetic acidHCID 12301—
ReactantHCID 178511295HCID 178511295—
ProductHCID 178468080HCID 178468080—

Reaction Steps

trans-N-{3-[4-Amino-5-(3-benzyloxy-phenyl)-pyrrolo[2,3-d]pyrimidin-7-yl]-cyclobutylmethyl}-2-ethoxy-acetamide is prepared starting from trans-7-(3-aminomethyl-cyclobutyl)-5-(3-benzyloxy-phenyl)-7H-pyrrolo[2,3-d]pyrimidin-4-ylamine and ethoxy-acetic acid (Fluka, Buchs, Switzerland) according to a procedure known in the art (M. Bodanszky in Principles of Peptide Synthesis, Akad.-Verlag, 1984). Analytical HPLC: tR=7.07 min (Grad 2); ES-MS: m/eo=486.2.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07326699B2
Source datasetuspto-grants-2008_02
ORD IDord-e186071c29c94ffa861c80c987f182f4
Source noteuspto-grants-2008_02