HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Toluenesulfonyl chloride → HCID 178435365, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | Piperidin-4-ol | HCID 79341 | — |
| Reactant | HCID 178435367 | HCID 178435367 | — |
| Product | HCID 178435365 | HCID 178435365 | — |
Reaction Steps
The title compound is prepared in analogy to Example 116 from cis-{3-[4-amino-5-(3-benzyloxy-phenyl)-6-ethyl-pyrrolo[2,3-d]pyrimidin-7-yl]-cyclobutyl}methanol of Example 124, p-toluenesulfonyl chloride and 4-hydroxypiperidine (Fluka, Buchs, Switzerland). Analytical HPLC-MS: tR=1.49 min; ES-MS: m/eo=512.48.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326699B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-e10744ac13f5400d8837f4fcf375f654 |
| Source note | uspto-grants-2008_02 |