HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Toluenesulfonyl chloride → HCID 178435364, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | Prolinol, (R)- | HCID 2724541 | — |
| Reactant | HCID 178435367 | HCID 178435367 | — |
| Product | HCID 178435364 | HCID 178435364 | — |
Reaction Steps
The title compound is prepared in analogy to Example 116 from cis-{3-[4-amino-5-(3-benzoyloxy-phenyl)-6-ethyl-pyrrolo[2,3-d]pyrimidin-7-yl]-cyclobutyl}-methanol of Example 124, p-toluenesulfonyl chloride and D-prolinol (Fluka, Buchs, Switzerland). Analytical HPLC-MS: tR=1.48 min; ES-MS: m/eo=512.48.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326699B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-5ccc241c184a40d49160584b14fd0450 |
| Source note | uspto-grants-2008_02 |