HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Tolylboronic acid → HCID 59654691, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Tolylboronic acid | HCID 2733950 | — |
| Reactant | (3-[(5-Bromo-furan-2-carbonyl)-amino]-phenyl)-acetic Acid Methyl Ester | HCID 59654700 | — |
| Product | HCID 59654691 | HCID 59654691 | — |
Reaction Steps
Methyl ester (16) (100 mg, 0.30 mmol) was coupled to 3-methyl-phenylboronic acid (44 mg, 0.33 mmol) using Method E. The crude compound was purified by column chromatography, eluting in 17% EtOAc in heptane to give the title compound. Yield: 20 mg, 19%; LC/MS tr 1.59 min; MS(ES+) m/z 350 (M+H)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326732B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-e8abde2055ff4ff7aafbbc03bc475b40 |
| Source note | uspto-grants-2008_02 |