HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2053149Generated: October 30, 2026
Phenylboronic Acid → HCID 59654761, compound
https://huagongshe.com/reaction/2053149
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | HCID 59654624 | HCID 59654624 | — |
| Product | HCID 59654761 | HCID 59654761 | — |
Reaction Steps
[3-(4-Bromo-2-methyl-benzoylamino)-phenyl]-acetic acid ethyl ester (188 mg, 0.50 mmol) was coupled to phenylboronic acid using Method E, except that the reaction mixture was heated at 80° C. The crude residue was purified by column chromatography using 20% EtOAc in heptane to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07326732B2 |
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| Source dataset | uspto-grants-2008_02 |
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| ORD ID | ord-b458d29b74004e8c9cfc4fea4f1e935c |
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| Source note | uspto-grants-2008_02 |
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