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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2053151Generated: October 30, 2026

Phenylboronic Acid → HCID 59654682, compound

https://huagongshe.com/reaction/2053151

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhenylboronic AcidHCID 66827—
ReactantHCID 59654821HCID 59654821—
ProductHCID 59654682HCID 59654682—

Reaction Conditions

Temperature80 °C

Reaction Steps

[3-(4-Bromo-2-chloro-benzoylamino)-phenyl]-acetic acid ethyl ester (198 mg, 0.50 mmol) was coupled to phenylboronic acid using Method E, except that the reaction mixture was heated at 80° C. The crude residue was purified by column chromatography using 20% EtOAc in heptane to give the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07326732B2
Source datasetuspto-grants-2008_02
ORD IDord-bb3edb7aa3404a36aae1bfc11e3119d7
Source noteuspto-grants-2008_02