HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2053155Generated: October 31, 2026
Phenylboronic Acid → HCID 59654817, compound
https://huagongshe.com/reaction/2053155
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | HCID 59654736 | HCID 59654736 | — |
| Product | HCID 59654817 | HCID 59654817 | — |
Reaction Steps
[3-(5-Bromo-2-fluoro-benzoylamino)-phenyl]-acetic acid ethyl ester (78) (209 mg, 0.55 mmol) was coupled to phenylboronic acid using Method E, except that the reaction mixture was heated at 80° C. The crude reside was purified by column chromatography using 20% EtOAc in heptane to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07326732B2 |
|---|
| Source dataset | uspto-grants-2008_02 |
|---|
| ORD ID | ord-5a6ebf43045943dea75177c7141a6b3b |
|---|
| Source note | uspto-grants-2008_02 |
|---|
