HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2053157Generated: November 1, 2026
Phenylboronic Acid → HCID 59654863, compound
https://huagongshe.com/reaction/2053157
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | [3-(3-Bromo-5-fluoro-benzoylamino)-phenyl]-acetic acid ethyl ester | HCID 59654737 | — |
| Product | HCID 59654863 | HCID 59654863 | — |
Reaction Steps
[3-(3-Bromo-5-fluoro-benzoylamino)-phenyl]-acetic acid ethyl ester (209 mg, 0.55 mmol) was coupled to phenylboronic acid using Method E, except that the reaction mixture was heated at 80° C. The crude residue was purified by column chromatography using 20% EtOAc in heptane to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07326732B2 |
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| Source dataset | uspto-grants-2008_02 |
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| ORD ID | ord-d177952213c7465689401bfd88e05b24 |
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| Source note | uspto-grants-2008_02 |
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