HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromobenzene → 2-Phenylfuran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromobenzene | HCID 7961 | — |
| Reactant | Furan-2-boronic acid | HCID 2734357 | — |
| Product | 2-Phenylfuran | HCID 519363 | — |
Reaction Steps
Bromobenzene (1.5 g, 9.55 mmol) was coupled to 2-furylboronic acid (1.75 g, 15.6 mmol) using Method E. The crude compound was purified by column chromatography using a stepped gradient of 5-10% EtOAc in heptane to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326732B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-ca01896ce3084ecf9117d00f367b9962 |
| Source note | uspto-grants-2008_02 |