Iodine → HCID 22716613, compound

HRID 2053334Notes

Reaction equation

[F:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[NH:8][CH2:9][C:10](O)=[O:11].[BH4-].[Na+].II>>[F:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[NH:8][CH2:9][CH2:10][OH:11]

Participants

Reactant 3

HCID 807Iodine

HCID 4311764Sodium borohydride

HCID 5171030N-o-Fluorophenylglycine

Product 1

HCID 22716613HCID 22716613, compound

Procedure

Similar procedure as described in example 31a) was used, starting from 2-fluorophenylglycine, sodium borohydride and iodine to give 2-fluoro-Phenylglycinol. LC-MS m/e 156 (MH+).

Sources & evidence

ORD record: ord-386e6f2a47db403ea9e4ea24408c2bf8
Source dataset: uspto-grants-2008_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07326786B2

Reaction notes

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