HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropanemethanamine → 2-(cyclopropylmethylamino)-1,3-thiazol-4-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropanemethanamine | HCID 75646 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | Rhodanine | HCID 1201546 | — |
| Product | 2-(cyclopropylmethylamino)-1,3-thiazol-4-one | HCID 178516938 | — |
Reaction Steps
Similar procedure as described in example 67(a) was used, starting from cyclopropylmethylamine, rhodanine (2-thioxo-4-thiazolidinone), mercuric chloride and DIEA to give 2-cyclopropylmethylamino-thiazol-4-one. LC-MS m/e 171 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326786B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-4cd0dd3c87aa47149edc8aac911469b2 |
| Source note | uspto-grants-2008_02 |