HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 3,4-Diphenyl-1,2,5-thiadiazole-1,1-dioxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Benzil | HCID 8651 | — |
| Reactant | Sulfamide | HCID 82267 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3,4-Diphenyl-1,2,5-thiadiazole-1,1-dioxide | HCID 11000109 | 84,416% |
Reaction Steps
Hydrogen chloride is bubbled through a solution of benzil (24 g, 0.11 mmol) and sulfamide (11 g, 0.11 mmol) in methanol (120 mL) for 2 h followed by heating to reflux for 2 h. The reaction mixture is cooled to RT, and the precipitate that formed is filtered to give 25.1 g of the product 14.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326792B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-18133539bc354892a6ad759e7691462d |
| Source note | uspto-grants-2008_02 |