HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 68571154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | cis-4,5-bis-(2-Bromophenyl)imidazolidine-2-thione | HCID 86596319 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68571154 | HCID 68571154 | 67.7% |
Reaction Steps
A solution of cis-4,5-bis-(2-bromophenyl)imidazolidine-2-thione (35) (0.51 g, 1.36 mmol) and methyl iodide (0.178 mL, 2.1 mmol) in abs. EtOH (20 mL) is heated at 90° C. overnight. The reaction mixture is cooled to rt, concentrated in vacuo, and the residue suspended in Et2O. The insoluble material is filtered to give 0.51 g of the product 52.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326792B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-5ddb561a0fbb4abe9f3fc81ad0c07319 |
| Source note | uspto-grants-2008_02 |