HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178464817, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | HCID 178464818 | HCID 178464818 | — |
| Product | HCID 178464817 | HCID 178464817 | 91% |
Reaction Steps
Prepared analogously to Example 17 from 4-(2-tert-butoxycarbonylaminomethyl-3-oxopiperazin-1-ylcarbonyl)-3-chloro-N-[1-(5-chloro-1H-benzimidazol-2-yl)ethyl]benzamide and trifluoroacetic acid. Yield: 91%; C22H22Cl2N6O3 (489.36); mass spectrum: (M+H)+=489/491/493 (chlorine isotope).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07326791B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-cc9197eaf0914c5cb33087794c647b0d |
| Source note | uspto-grants-2008_02 |