HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrafluoro-m-phenylenediamine dihydrochloride → n-(3-Methylpyrid-2-yl)benzene-1,4-diamine dihydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrafluoro-m-phenylenediamine dihydrochloride | HCID 149026 | — |
| Reactant | 3-methyl-N-(4-nitrophenyl)pyrid-2-amine | HCID 23104477 | — |
| Catalyst | ZINC ammonium chloride water ethanol | HCID 131726756 | — |
| Product | n-(3-Methylpyrid-2-yl)benzene-1,4-diamine dihydrochloride | HCID 69201221 | — |
Reaction Steps
The 3-methyl-N-(4-nitrophenyl)pyrid-2-amine (7) obtained above was reduced with a boiling zinc/ammonium chloride/water/ethanol mixture. The corresponding amine was isolated in dihydrochloride form.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07329288B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-8dd0389b0db341d5b62d3d8f4cebcbf6 |
| Source note | uspto-grants-2008_02 |