HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroacetophenone → HCID 67213258, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroacetophenone | HCID 10757 | — |
| Reactant | 1-(2-Chlorophenyl)-4,4,4-trifluorobutane-1,3-dione | HCID 15772022 | — |
| Reactant | HCID 178510443 | HCID 178510443 | — |
| Product | HCID 67213258 | HCID 67213258 | 23% |
Reaction Steps
Reaction of 1-(2-chloro-phenyl)-4,4,4-trifluoro-butane-1,3-dione (251 mg, 1.0 mmol), prepared from commercially available 2-chloro-acetophenone according to general procedure A, and 3-amino-4-cyano-pyrazole (108 mg, 1.0 mmol) according to general procedure B yielded the title compound as an off-white solid (73 mg, 23%). MS (ISP) 323.1 [(M+H)+]; mp 169° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07329662B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-287bc603182040ddbb35aa06f2a22d91 |
| Source note | uspto-grants-2008_02 |