HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,4,4-Trifluoro-1-(3-fluorophenyl)butane-1,3-dione → HCID 67213091, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,4,4-Trifluoro-1-(3-fluorophenyl)butane-1,3-dione | HCID 43186918 | — |
| Reactant | HCID 178510443 | HCID 178510443 | — |
| Product | HCID 67213091 | HCID 67213091 | 46% |
Reaction Steps
Reaction of 1-(3-fluoro-phenyl)-4,4,4-trifluoro-butane-1,3-dione (234 mg, 1.0 mmol), prepared from commercially available 3-fluoro-acetophenone according to general procedure A, and 3-amino-4-cyano-pyrazole (108 mg, 1.0 mmol) according to general procedure B yielded the title compound as a light yellow solid (141 mg, 46%). MS (ISP) 306.9 [(M+H)+]; mp 199° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07329662B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-ec83cb71386549b69b1f934f44a1c0c2 |
| Source note | uspto-grants-2008_02 |