HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86598655, compound → HCID 11428764, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86598655 | HCID 86598655 | — |
| Reactant | HCID 178510443 | HCID 178510443 | — |
| Product | HCID 11428764 | HCID 11428764 | 38.5% |
Reaction Steps
Reaction of 1-(4-fluoro-3-trifluoromethyl-phenyl)-4,4,4-trifluoro-butane-1,3-dione (302 mg, 1.0 mmol), prepared from commercially available 4-fluoro3-trifluoromethyl-acetophenone according to general procedure A, and 3-amino-4-cyano-pyrazole (108 mg, 1.0 mmol) according to general procedure B yielded the title compound as an off-white solid (144 mg, 38%). MS (ISP) 375.0 [(M+H)+]; mp 204° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07329662B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-39b97ce39cb2417687bd1af59e75c9c0 |
| Source note | uspto-grants-2008_02 |