Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,3-Butanedione, 1-(4-chloro-3-methylphenyl)-4,4,4-trifluoro- → HCID 11395130, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,3-Butanedione, 1-(4-chloro-3-methylphenyl)-4,4,4-trifluoro- | HCID 67000978 | — |
| 반응물 | HCID 178509259 | HCID 178509259 | — |
| 생성물 | HCID 11395130 | HCID 11395130 | 75% |
반응 단계
Reaction of 1-(4-chloro-3-methyl-phenyl)-4,4,4-trifluoro-butane-1,3-dione (132 mg, 0.5 mmol), prepared from commercially available 4-chloro-3-methyl-acetophenone according to general procedure A, and 3-amino-4-(4-pyridinyl)-pyrazole [CAS No. 216661-87-9; prepared from 4-cyanomethyl-pyridine as described in Bioorg. Med. Chem. Lett. 12 (2002) 3537-3541] (80 mg, 0.5 mmol) according to general procedure B yielded the title compound as a yellow solid (145 mg, 75%). MS (ISP) 389.2 [(M+H)+]; mp 247° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07329662B2 |
| 출처 데이터셋 | uspto-grants-2008_02 |
| ORD ID | ord-a38039090b2b43a1a55748a1f32be3bb |
| 출처 메모 | uspto-grants-2008_02 |