HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Chlorophenyl)ethanone → HCID 11313301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Chlorophenyl)ethanone | HCID 14933 | — |
| Reactant | 5-amino-1H-imidazole-4-carbonitrile | HCID 78777 | — |
| Reactant | 1-(3-Chlorophenyl)-4,4,4-trifluorobutane-1,3-dione | HCID 15338012 | — |
| Product | HCID 11313301 | HCID 11313301 | 41.2% |
Reaction Steps
Reaction of 1-(3-chloro-phenyl)-4,4,4-trifluoro-butane-1,3-dione (251 mg, 1.0 mmol), prepared from commercially available 3-chloro-acetophenone according to general procedure A, and 4-amino-5-cyano-1H-imidazole (108 mg, 1.0 mmol) according to general procedure B yielded the title compound as a yellow solid (133 mg, 41%). MS (ISP) 323.1 [(M+H)+]; mp 221° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07329662B2 |
| Source dataset | uspto-grants-2008_02 |
| ORD ID | ord-a3fc7c16b80b4997a0da37330135735c |
| Source note | uspto-grants-2008_02 |